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資訊中心

07.24

2012

納米材料和生物材料進行樣品測試時如何選擇支持膜？

第一次選購或使用碳支持膜的朋友，往往不知道選用哪種目數的銅網支持膜合適。

07.23

2012

TEM粉末樣品的制備方法

取少量待觀察的粉末顆粒，放入潔凈的小燒杯或試管中

07.23

2012

TEM金屬薄膜樣品的制備方法

用線切割機將樣品切割成0.5~1mm薄片。

07.23

2012

薄膜材料包埋的技術要點

對于硬材料如半導體、薄膜、多層膜等材料而言，進行超薄切片之前的包埋過程是非常重要的，尤其是對于需要確定方向的多層膜材料。

07.23

2012

常溫超薄切片操作步驟

材料的超薄切片制樣方法主要分為硬材料的室溫切片過程和軟材料的冷凍切片過程兩大類

07.23

2012

如何確定SAED晶帶軸？

晶帶軸是兩個衍射斑點矢量的叉積，符合右手定則。斑點對應的晶面是包含帶軸的。

07.23

2012

微乳制劑做電鏡如何制樣

電鏡要求高真空狀態,液體不合適，可以利用具有冷凍功能的電鏡(CRYO-TEM)做。

07.23

2012

透射電鏡踩正晶帶軸方法和步驟

最常用的方法是利用電子衍射，把衍射圖調整得對稱，帶軸就比較正了。看到的對稱性和你的晶體類型已經使用的衍射方式有關。

07.23

2012

TEM樣品的制備工藝流程和注意事項

將所測樣品在金剛砂紙上磨薄，然后用AB膠粘在銅環上，將粘好的樣品放入離子減薄機中進行離子減薄至樣品被打穿，并出現薄區為止

07.23

2012

超薄切片在材料科學電鏡制樣上的應用

超薄切片

在線商城

聯系電話

在線客服

納米材料和生物材料進行樣品測試時如何選擇支持膜？

第一次選購或使用碳支持膜的朋友，往往不知道選用哪種目數的銅網支持膜合適。

取少量待觀察的粉末顆粒，放入潔凈的小燒杯或試管中

用線切割機將樣品切割成0.5~1mm薄片。

對于硬材料如半導體、薄膜、多層膜等材料而言，進行超薄切片之前的包埋過程是非常重要的，尤其是對于需要確定方向的多層膜材料。

如何確定SAED晶帶軸？

晶帶軸是兩個衍射斑點矢量的叉積，符合右手定則。斑點對應的晶面是包含帶軸的。

電鏡要求高真空狀態,液體不合適，可以利用具有冷凍功能的電鏡(CRYO-TEM)做。

最常用的方法是利用電子衍射，把衍射圖調整得對稱，帶軸就比較正了。看到的對稱性和你的晶體類型已經使用的衍射方式有關。

將所測樣品在金剛砂紙上磨薄，然后用AB膠粘在銅環上，將粘好的樣品放入離子減薄機中進行離子減薄至樣品被打穿，并出現薄區為止